名称:(4-甲氧苯基)肼盐酸盐
英文名称:(4-methoxybenzyl)hydrazine dihydrochloride
分子式:c8h14cl2n2o

分子量: 225.12
cas no.:2011-48-5
结构式:image.png

规格:95%

用途:基础原料、有机中间体、医药中间体

合成路线如下:

hydrogenchloride; hydrazine hydrate; ethanol;

reactants are commercially availlable.
parratt, martin john, us2003/18197, a1, (2003) a solution containing 7.9 ml of hydrazine hydrate in 80 ml of ethanol was treated with 3.7 ml of 4-m ethoxybenzylchloride and heated at 90°c. for 2.0 h. the solvent was reduced by evaporation under re duced pressure and then the resulting residue was dissolved in 30 ml of ethanol. the solution was ac idified with 30 ml of 5n hcl at 0°c. and a white precipitate separated. the white solid was filtere d off and dried to give 2.75 g of (4-methoxybenzyl)hydrazine dihydrochloride (pmbnhnh2.2hcl), which was used without further purification.


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